OpenARCHEM

Agilent 6890N Network 6C

OpenARCHEM Id:
oa2017equ3
Manufacturer:
Agilent
Model:
6890N Network 6C
Column manufacturer:
Column model:
Detector:
Agilent 5973N Network Mass Selective
Settings:
capillary column (30.0 m x 250 mm x 0.15 mm) set to constant flow mode and front inlet. The carrier gas flow (helium) was set to 0.5 ml/min with an average velocity of 41cm/sec. The EPC Split-Splitless Inlet was set to splitless. The GC oven temperature had a set point of 110 degrees Celsius held for 2 minutes and increased by 6 degrees a minute until it hit 250 degrees and then held for 20 minutes
Notes:
Samples were automatically injected with an Agilent Technologies 7683 Series Injector with 10μl syringe; 1μl was injected for most samples with the exception of runs starting from the 12th one, which had 2μl injections; Before the injection of each sample, the computer automatically cleaned the syringe with 10μl of methylene chloride twice and also primed it twice with the ORA sample pre-injection. Post-injection, the syringe was cleaned four times using 10μl of methylene chloride